Pyrolysis, deconvolution

Pyrolysis: deconvolution

Estimates parameters in pyrolysis DTG UNDER CONSTRUCTION

2024.Jul.03 13:28:24

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##TempC;DTG;;
29,55833244;0,042734146;-5,9765625;78,890625
29,55997658;0,050479889;-7,2734375;78,890625
29,56027031;0,057975769;-8,58203125;79,1015625
29,57484436;0,061433792;-9,91796875;79,0078125
29,59329605;0,06546402;-11,2421875;79,4296875
29,60457802;0,082668304;-12,55859375;79,8515625
29,6187973;0,101234436;-13,87890625;79,96875
29,61950111;0,132471085;-15,22460938;79,1484375
29,61327362;0,174100876;-16,57617188;77,8828125
29,60369682;0,228017807;-17,87890625;76,265625
29,60122871;0,283817291;-19,11132813;74,6484375
29,60686874;0,344949722;-20,30664063;73,171875
29,64076996;0,401165009;-21,51171875;72,9140625
29,70056725;0,452810287;-22,73242188;73,3359375
29,76522446;0,5091362;-23,95117188;73,828125
29,84623909;0,561855316;-25,18945313;74,296875
29,91754532;0,625793457;-26,43164063;74,578125
29,98489952;0,696165085;-27,69335938;74,6484375
30,0311203;0,779655457;-28,93359375;74,6015625
30,08683205;0,861183167;-30,1796875;74,53125
30,13016129;0,952976227;-31,41796875;74,109375
30,18391418;1,041246414;-32,65429688;73,8984375
30,2423439;1,129432678;-33,88085938;73,5
30,3117733;1,213209152;-35,10351563;73,5234375
30,39213181;1,293439865;-36,3203125;73,21875
30,48704147;1,367221832;-37,53710938;73,40625
30,57728767;1,445486069;-38,765625;73,5
30,67112732;1,523235321;-39,984375;73,9453125
30,76627541;1,60153389;-41,21484375;74,0625
30,86483192;1,677564621;-42,47070313;74,6953125
30,95762253;1,757310867;-43,70703125;74,9296875
31,06229019;1,830533981;-44,96484375;75,3046875
31,1686058;1,902130127;-46,21679688;75,7734375
31,28344917;1,9718647;-47,48632813;76,2421875
31,38400841;2,044933319;-48,75976563;76,59375
31,48767281;2,116857529;-50,046875;77,296875
31,59391403;2,189888;-51,3359375;77,8828125
31,70534897;2,261327744;-52,63671875;78,65625
31,83320618;2,324102402;-53,94921875;79,2890625
31,96838379;2,385055542;-55,27539063;79,96875
32,1085434;2,444480896;-56,609375;80,7890625
32,24455261;2,506622314;-57,96875;81,375
32,39000702;2,563365936;-59,33398438;82,0078125
32,52638245;2,623434067;-60,69726563;82,734375
32,67648315;2,676919937;-62,08789063;83,625
32,82509995;2,730953217;-63,48046875;84,2109375
32,97495651;2,782693863;-64,89648438;85,0546875
33,11823654;2,837940216;-66,31835938;85,6171875
33,27069092;2,888801575;-67,75390625;86,3203125
33,42455292;2,938838959;-69,19335938;86,953125
33,57184219;2,9936409;-70,64257813;87,796875
33,73140717;3,042598724;-72,125;88,640625
33,90356064;3,083978653;-73,60351563;89,671875
34,06428909;3,130783081;-75,10742188;90,6328125
34,22133636;3,181013107;-76,6328125;91,3125
34,40322495;3,217573166;-78,15625;92,0390625
34,58423233;3,253139496;-79,69726563;92,859375
34,75371552;3,293935776;-81,24804688;93,5859375
34,93946457;3,326688766;-82,81445313;94,453125
35,12765503;3,357219696;-84,40039063;95,671875
35,30296326;3,393302917;-86,00195313;96,75
35,48961639;3,423877716;-87,62109375;97,734375
35,69876099;3,443365097;-89,25585938;98,8359375
35,90142822;3,464025497;-90,91601563;99,703125
36,1041069;3,483602524;-92,58984375;100,78125
36,30370331;3,50535965;-94,2734375;101,8828125
36,49155045;3,533290863;-95,97265625;103,0546875
36,67639923;3,563524246;-97,70507813;104,015625
36,86978149;3,588504791;-99,44921875;105,375
37,07030869;3,609615326;-101,2089844;106,4296875
37,27625275;3,629152298;-102,9921875;107,71875
37,48771667;3,644989014;-104,7910156;108,984375
37,70173264;3,655776978;-106,6289063;110,671875
37,9161377;3,668796539;-108,4804688;112,0546875
38,12355042;3,684963226;-110,3652344;113,3671875
38,33901215;3,693016052;-112,2695313;114,5859375
38,56426239;3,696123123;-114,1914063;116,0390625
38,7956543;3,697973251;-116,1328125;117,2109375
39,01874924;3,703022003;-118,09375;118,5
39,24785995;3,7035923;-120,0839844;119,8828125
39,48060989;3,702440262;-122,0878906;121,453125
39,69673538;3,70838356;-124,1269531;122,765625
39,91741562;3,708812714;-126,1855469;124,265625
40,14741898;3,703790665;-128,2636719;125,6953125
40,38261795;3,695337296;-130,3789063;127,546875
40,62743378;3,682807922;-132,5;128,9296875
40,87336731;3,669670105;-134,6679688;130,7109375
41,11632156;3,657596588;-136,8691406;132,234375
41,36549377;3,644359589;-139,0878906;133,9921875
41,61644363;3,627779007;-141,3300781;135,4921875
41,85333633;3,611694336;-143,5917969;137,2734375
42,1111412;3,583610535;-145,9042969;139,125
42,37376785;3,553936005;-148,234375;140,953125
42,62414551;3,526935577;-150,6015625;143,0859375
42,87361908;3,500850677;-153,0058594;144,8671875
43,12702942;3,475625992;-155,4296875;147,0234375
43,37992096;3,446643829;-157,9082031;148,921875
43,63562775;3,414907455;-160,3984375;151,171875
43,89908218;3,378194809;-162,9335938;152,953125
44,17885208;3,331319809;-165,4960938;155,1796875
44,45278931;3,286762238;-168,1015625;157,03125
44,727005;3,246006012;-170,7363281;159,046875
44,99436188;3,207845688;-173,40625;160,9921875
45,27045441;3,163986206;-176,0996094;163,0546875
45,53385544;3,127281189;-178,8378906;165,140625
45,80019379;3,086772919;-181,6152344;167,4375
46,07662201;3,037338257;-184,4179688;169,8046875
46,35645676;2,984449387;-187,265625;172,1015625
46,63666153;2,929193497;-190,1503906;174,703125
46,91581345;2,869132996;-193,0859375;177,1640625
47,20487976;2,804666519;-196,0625;179,6484375
47,4822464;2,747991562;-199,0703125;182,0625
47,76459122;2,686628342;-202,1210938;184,5234375
48,04872131;2,623809814;-205,2128906;186,7265625
48,35003281;2,553186417;-208,359375;189,1640625
48,64354706;2,486413956;-211,5273438;191,71875
48,94029236;2,417715073;-214,7402344;194,3671875
49,23623276;2,349733353;-217,9941406;196,8984375
49,52957535;2,280277252;-221,3066406;199,828125
49,82239914;2,208457947;-224,6640625;202,546875
50,11290741;2,135625839;-228,0625;205,171875
50,41308975;2,056755066;-231,5058594;207,7265625
50,71679688;1,971038818;-234,9921875;210,3984375
51,02494049;1,886945724;-238,5097656;212,765625
51,33188248;1,804103851;-242,078125;215,34375
51,63741684;1,721227646;-245,6933594;217,8046875
51,94919968;1,635248184;-249,3457031;220,3359375
52,25930023;1,555961609;-253,0332031;223,03125
52,55873489;1,477491379;-256,7695313;225,75
52,85270309;1,400350571;-260,5546875;228,421875
53,15903854;1,313657761;-264,390625;231,1640625
53,47009277;1,222736359;-268,2695313;233,953125
53,78161621;1,123250961;-272,1855469;236,6015625
54,10345459;1,024583817;-276,1425781;239,3203125
54,42654037;0,920610428;-280,1621094;242,0859375
54,74804306;0,818696976;-284,2128906;245,0390625
55,05826187;0,723953247;-288,3164063;248,015625
55,37417221;0,626974106;-292,4765625;250,8984375
55,69927216;0,521730423;-296,6992188;254,015625
56,02268219;0,41768074;-300,953125;257,0625
56,34999084;0,311481476;-305,2558594;259,9453125
56,6842041;0,197359085;-309,6132813;262,6171875
57,01709366;0,088453293;-314,0214844;265,6875
57,34913254;-0,023902893;-318,46875;268,5
57,68582535;-0,136980057;-322,9589844;271,3359375
58,01570511;-0,242921829;-327,5078125;274,1015625
58,3490181;-0,346010208;-332,0976563;276,9375
58,67743301;-0,445365906;-336,7363281;279,75
59,00859833;-0,544155121;-341,4355469;282,328125
59,34208298;-0,643655777;-346,1601563;284,90625
59,67924881;-0,745025635;-350,9335938;287,6484375
60,0133667;-0,8515625;-355,734375;290,2734375
60,35199738;-0,965272903;-360,59375;292,828125
60,69825745;-1,080545425;-365,5039063;295,5703125
61,04889297;-1,196315765;-370,4609375;298,3828125
61,40027618;-1,314668655;-375,4472656;300,984375
61,74484634;-1,425798416;-380,4960938;303,84375
62,08783722;-1,53338623;-385,5761719;306,5625
62,42748642;-1,646520615;-390,7148438;309,28125
62,77133942;-1,755048752;-395,890625;311,8359375
63,12276459;-1,858119965;-401,1054688;314,6015625
63,48246002;-1,957128525;-406,3730469;317,296875
63,852211;-2,062759399;-411,6796875;319,734375
64,21568298;-2,166399002;-417,0371094;322,171875
64,5633316;-2,262500763;-422,4238281;324,84375
64,90978241;-2,362644196;-427,859375;327,1640625
65,26771545;-2,468233109;-433,3261719;329,3671875
65,62870026;-2,570596695;-438,8476563;331,546875
65,98429108;-2,667604446;-444,3945313;333,8203125
66,34802246;-2,763917923;-449,9746094;335,8476563
66,72207642;-2,864683151;-455,5917969;337,828125
67,0827713;-2,967002869;-461,2412109;339,8671875
67,44506836;-3,064558029;-466,9189453;341,8710938
67,80701447;-3,14304924;-472,6298828;343,7109375
68,16640472;-3,214832306;-478,3828125;345,4921875
68,52770996;-3,280002594;-484,1552734;347,34375
68,89897156;-3,344852448;-489,9511719;348,9960938
69,27429199;-3,412841797;-495,7910156;350,6132813
69,65763855;-3,494901657;-501,640625;352,3007813
70,04903412;-3,579559326;-507,5283203;353,8945313
70,4343338;-3,658315659;-513,4335938;355,4296875
70,81198883;-3,718017578;-519,3828125;356,8359375
71,18495941;-3,763805389;-525,3427734;358,2773438
71,56237793;-3,800598145;-531,3154297;359,5078125
71,94947815;-3,833972931;-537,3242188;360,4570313
72,33765411;-3,865797043;-543,3388672;361,5585938
72,72608948;-3,90712738;-549,3769531;362,4960938
73,11241913;-3,956628799;-555,4238281;363,3984375
73,50309753;-4,003446579;-561,4873047;364,1484375
73,89814758;-4,055892944;-567,5634766;365,1210938
74,28712463;-4,087060928;-573,6660156;365,6953125
74,68774414;-4,100942612;-579,7734375;366,375
75,09346008;-4,101051331;-585,8867188;367,1835938
75,48574066;-4,089107513;-591,9990234;367,5234375
75,86804199;-4,074110031;-598,1376953;367,7929688
76,26289368;-4,074668884;-604,2744141;368,0859375
76,67346191;-4,088499069;-610,4111328;368,0039063
77,08164978;-4,09651947;-616,5361328;367,7695313
77,49081421;-4,089820862;-622,6669922;367,7695313
77,90690613;-4,070386887;-628,7978516;367,5585938
78,32548523;-4,051971436;-634,9228516;367,40625
78,71972656;-4,008399963;-641,0478516;367,1132813
79,12294006;-3,962152481;-647,1650391;366,8203125
79,53663635;-3,92773056;-653,2783203;366,1523438
79,95162964;-3,87733078;-659,3789063;365,6953125
80,35720825;-3,814325333;-665,4658203;364,7460938
80,78126526;-3,746852875;-671,5351563;364,1484375
81,21427155;-3,671821594;-677,6035156;363,1757813
81,64479828;-3,584114075;-683,6484375;362,15625
82,07083893;-3,487133026;-689,6865234;361,0664063
82,50344849;-3,36904335;-695,6816406;359,7539063
82,93520355;-3,24221611;-701,6845703;358,265625
83,35617828;-3,110816956;-707,6386719;356,71875
83,77661896;-2,966745377;-713,5654297;355,4648438
84,20523071;-2,83042717;-719,4804688;353,8007813
84,63153839;-2,684408188;-725,3652344;352,3945313
85,06915283;-2,537561417;-731,2304688;350,9296875
85,51345825;-2,392076492;-737,0654297;349,171875
85,94950867;-2,22986412;-742,8720703;347,109375
86,39354706;-2,04535675;-748,6328125;345,0117188
86,84293365;-1,868276596;-754,3710938;343,0195313
87,29009247;-1,684936523;-760,0722656;340,7460938
87,73493958;-1,473758698;-765,7304688;338,6132813
88,18569183;-1,256931305;-771,3642578;336,3984375
88,63798523;-1,045713425;-776,9492188;334,1015625
89,09819031;-0,817922592;-782,5029297;331,5820313
89,54402161;-0,577007294;-788,0126953;329,203125
89,99203491;-0,332756042;-793,4736328;326,625
90,44698334;-0,093307495;-798,890625;323,8945313
90,91040802;0,15823555;-804,2841797;321,1757813
91,36620331;0,421152115;-809,6044922;318,3867188
91,8399353;0,689176559;-814,8808594;315,234375
92,31497192;0,958255768;-820,1162109;312,140625
92,79281616;1,243499756;-825,2890625;309,1523438
93,26346588;1,541791916;-830,4248047;305,9882813
93,73365021;1,850391388;-835,4951172;302,8242188
94,20180511;2,167089462;-840,515625;299,5898438
94,66984558;2,493562698;-845,4794922;296,2148438
95,13244629;2,830091476;-850,3955078;292,6640625
95,59580231;3,177093506;-855,25;289,125
96,06690979;3,523944855;-860,03125;285,3046875
96,53842163;3,878993988;-864,7568359;281,4726563
97,01013947;4,248661041;-869,4267578;277,6289063
97,49203491;4,62657547;-874,0107422;273,796875
97,97722626;5,009529114;-878,546875;269,8359375
98,46881104;5,39921093;-883,0078125;265,7109375
98,96164703;5,792487144;-887,4140625;261,7382813
99,45648193;6,186989784;-891,7412109;257,765625
99,93980408;6,590779305;-896,0009766;253,6640625
100,425087;6,997959137;-900,1923828;249,4804688
100,9156647;7,405356407;-904,3300781;245,3554688
101,4015579;7,824069023;-908,375;241,2539063
101,8874969;8,257884026;-912,359375;236,90625
102,3808594;8,694346428;-916,2705078;232,8515625
102,8810501;9,1340065;-920,1123047;228,7851563
103,3710327;9,584217072;-923,8935547;224,8125
103,8634644;10,03646278;-927,6074219;220,7460938
104,3568726;10,48748016;-931,2646484;216,9375
104,8462372;10,94518089;-934,8320313;212,8828125
105,3504715;11,40294266;-938,3554688;208,9921875
105,8600006;11,86522865;-941,7998047;205,0898438
106,3666611;12,3332634;-945,1884766;201,1171875
106,8682632;12,81028175;-948,5039063;197,1445313
107,3871841;13,28064156;-951,7568359;193,2539063
107,8919067;13,75900269;-954,9501953;189,4335938
108,3825302;14,24780273;-958,0683594;185,53125
108,8855286;14,73743868;-961,1337891;181,7109375
109,399292;15,22683525;-964,1298828;177,8085938
109,9129181;15,72259521;-967,0527344;173,9648438
110,420372;16,22365761;-969,9267578;170,0507813
110,9414368;16,72078609;-972,7265625;166,2304688
111,465332;17,21745753;-975,4580078;162,6328125
111,9879761;17,71765995;-978,1416016;159,1757813
112,5048294;18,21944833;-980,7587891;155,6601563
113,0254211;18,72130847;-983,3330078;152,0625
113,5409164;19,22681832;-985,8388672;148,5351563
114,0504303;19,73690784;-988,2890625;144,9140625
114,5546646;20,24939924;-990,6669922;141,3046875
115,061615;20,76576543;-992,9941406;137,7070313
115,5738525;21,2809469;-995,2548828;134,4609375
116,0940323;21,79163998;-997,4667969;131,2851563
116,6190948;22,30086541;-999,6298828;128,1328125
117,1469193;22,8101747;-1001,742188;124,8164063
117,6637344;23,3208344;-1003,800781;121,8515625
118,1776047;23,83210135;-1005,797852;118,6171875
118,6951904;24,34191418;-1007,745117;115,6054688
119,2039032;24,85455823;-1009,643555;112,5117188
119,7142258;25,36545944;-1011,504883;109,5
120,239296;25,8713212;-1013,305664;106,4882813
120,7600784;26,37658739;-1015,057617;103,8515625
121,2747116;26,88438749;-1016,74707;101,1210938
121,7980042;27,38702965;-1018,413086;98,61328125
122,3170242;27,88821411;-1020,036133;96,31640625
122,8330002;28,38912868;-1021,62207;93,73828125
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597,9156494;64,4304142;-8786,05957;48,60351563
598,2572632;63,81494713;-8786,86377;47,81835938
598,5849609;63,20169258;-8787,655273;46,56445313
598,9092407;62,57999992;-8788,446289;44,75976563
599,2169189;61,94305611;-8789,185547;42,36914063
599,5271606;61,29327965;-8789,864746;39,515625
599,8251953;60,63682747;-8790,506836;36,59179688
600,1376343;59,97753716;-8791,07373;33,15820313
600,4108887;59,37521935;-8791,624023;30,04101563
600,6307373;58,90641594;-8792,09375;26,54882813

Final mass, ashes

In sample.

Initial guesses

xtol, ftol, maxiter

(-1 → 2500×#guesses)

Tolerances for x, y; max. iterations.

Show values

Show graph coordinates.

# VERIF From Excel file (uploaded '.xlsx' or inserted '.csv'), computes the parameters for the pseudo-Gaussians, in a TG experiment, from the DTG data, and computes the compositions (4 in the base data, with 2.nd to 4.th: hemicellulose, cellulose, lignin).
^(a) Thus, n = 4 components.

The base 'csv' data lead to a run time of #~4 s, as well as the suggested 'xlsx' (which is the same). (For security, / is not allowed in the data.)

References:

Plate: DTGdeConv

• Google: Thermogravimetry

• (Wikipedia) Thermogravimetric analysis.

• 1698-09-28: Maupertuis, Pierre Louis Moreau de (†1759-07-27, 60 yrs.).

http://web.tecnico.ulisboa.pt/~mcasquilho/compute/com/,pyrolysis/P-pyroDeconv.php
Created: 2024-05-19 — Last modified: 2024-05-21